potassium carbonate in acetone
T=25°C; 20 h; Heating / reflux;
参考文献
Aslanian, Robert; Zhu, Xiaohong; Vaccaro, Henry A.; Shih, Neng-Yang; Piwinski, John J.; Williams, Shirley M.; West Jr., Robert E.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 18 p. 5032 - 5036
1: With pyridine in dichloromethane
T=0 - 20°C; Inert atmosphere;
2: With water; sodium hydrogencarbonate in dichloromethane
1 h; Saturated solution;
3: With hydrogenchloride in water
pH=5;
参考文献
Babtie, Ann C.; Bandyopadhyay, Subhajit; Olguin, Luis F.; Hollfelder, Florian
Angewandte Chemie, International Edition, 2009 , vol. 48, # 20 p. 3692 - 3694
