1: With copper(l) chloride in various solvent(s) T=20°C; Reduction; Coupling; Silylation; 24 h; 2: With water; toluene-4-sulfonic acid in various solvent(s) T=20°C; Hydrolysis;
(2,6-t-Bu2-4-Me-C6H2O)2AlMe; diisobutylaluminium hydride T=-78°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Maruoka, Keiji; Araki, Yoshitaka; Yamamoto, Hisashi
Journal of the American Chemical Society, 1988 , vol. 110, # 8 p. 2650 - 2652