4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C; 5 h; Inert atmosphere;
参考文献
Hwang, Soonho; Choi, Sang Yoon; Lee, Jin Hee; Kim, Shinae; In, Jinkyung; Ha, Sang Keun; Lee, Eunjung; Kim, Tae-Yoon; Kim, Sun Yeou; Choi, Sun; Kim, Sanghee
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 15 p. 5602 - 5609
1: in acetonitrile
T=80°C;
2: With polymer supported NaCO3 in acetonitrile
Further stages.;
参考文献
Smith, Christopher D.; Baxendale, Ian R.; Tranmer, Geoffrey K.; Baumann, Marcus; Smith, Stephen C.; Lewthwaite, Russell A.; Ley, Steven V.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 10 p. 1562 - 1568
1.1: NaH / tetrahydrofuran
1.2: 100 percent / tetrahydrofuran / 0.5 h / 20 °C
2.1: 96 percent / tetrahydrofuran / 4 h / Heating
View Scheme
参考文献
Sammes,P.G.
Journal of the Chemical Society, 1965 , p. 6608 - 6613
→
反应条件
in acetonitrile
T=80°C; Title compound not separated from byproducts.;
参考文献
Smith, Christopher D.; Baxendale, Ian R.; Tranmer, Geoffrey K.; Baumann, Marcus; Smith, Stephen C.; Lewthwaite, Russell A.; Ley, Steven V.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 10 p. 1562 - 1568
