1: 83 percent / AlCl3 / CH2Cl2 / 2.33 h / 10 - 20 °C
2: 79 percent / pyridine; KMnO4 / H2O / 5 h / Heating
View Scheme
参考文献
Hibbs, Michael R.; Vargas, Marian; Holtzclaw, Jeremy; Rich, Wendy; Collard, David M.; Schiraldi, David A.
Macromolecules, 2003 , vol. 36, # 20 p. 7543 - 7551
1: vinyl ethyl ketone With indium(III) chloride; indium in water; acetonitrile
T=20°C; 24 h;
2: 4-methoxy-benzoyl chloride With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
24 h; Reflux;
参考文献
Shen, Zhi-Liang; Goh, Kelvin Kau Kiat; Cheong, Hao-Lun; Wong, Colin Hong An; Lai, Yin-Chang; Yang, Yong-Sheng; Loh, Teck-Peng
Journal of the American Chemical Society, 2010 , vol. 132, # 45 p. 15852 - 15855
1: in benzene
T=30°C; 3 h;
2: With sodium hydroxide in benzene
T=20°C; 0.5 h;
参考文献
Toriyama, Masaharu; Kamijo, Haruo; Motohashi, Shigeyasu; Takido, Toshio; Itabashi, Kunio
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 8 p. 1661 - 1665
