4-Methylpyridine; di-tert-butyl dicarbonate; lithium chloride; palladium dichloride in 1-methyl-pyrrolidin-2-one
T=120°C; Heck olefination; 16 h; Title compound not separated from byproducts;
参考文献
Goossen, Lukas J.; Paetzold, Jens; Winkel, Lars
Synlett, 2002 , # 10 p. 1721 - 1723
1: 4-methoxy-benzoic acid With 1,1'-carbonyldiimidazole in tetrahydrofuran
1 h; RefluxInert atmosphere;
2: aci-anion nitromethane sodium salt in tetrahydrofuran; mineral oil
16 h; RefluxInert atmosphere;
参考文献
Lindsay, Vincent N. G.; Lin, Wei; Charette, Andre B.
Journal of the American Chemical Society, 2009 , vol. 131, # 45 p. 16383 - 16385