1: With potassium carbonate Horner-Wadsworth-Emmons olefination; 6 h; Neat (no solvent)high-speed ball milling; 2: With Oxonereg; 12 h; Neat (no solvent)high-speed ball milling; optical yield given as percent dediastereoselective reaction;
参考文献
Shearouse, William C.; Korte, Chelsea M.; Mack, James
Green Chemistry, 2011 , vol. 13, # 3 p. 598 - 601
in water T=65°C; P=750060 Torr; 66 h; further p-substituted benzenediazonium tetrafluoroborates; variation of temperature , time, and pressure; field and resonance reaction constants; Product distributionMechanism;
参考文献
Ravenscroft, Michael D.; Skrabal, Peter; Weiss, Bettina; Zollinger, Heinrich
Helvetica Chimica Acta, 1988 , vol. 71, p. 515 - 520
