1-(氯甲基)-4-硝基苯合成路线 (共 349 条)
反应条件
sodium hydride in N,N-dimethyl-formamide
参考文献
Broxton; Morrison
Australian Journal of Chemistry, 1985 , vol. 38, # 7 p. 1037 - 1043
反应条件
sodium carbonate; trans-PdBr(N-Succ)(PPh3)2 in tetrahydrofuran T=80°C; Suzuki-Miyaura cross-coupling; 3 h;
参考文献
Burns, Michael J.; Fairlamb, Ian J. S.; Kapdi, Anant R.; Sehnal, Petr; Taylor, Richard J. K.
Organic Letters, 2007 , vol. 9, # 26 p. 5397 - 5400
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; palladium diacetate in 1,4-dioxane T=80°C; Stille cross-coupling; 3 h;
参考文献
Nichele, Tatiana Z.; Monteiro, Adriano L.
Tetrahedron Letters, 2007 , vol. 48, # 42 p. 7472 - 7475
反应条件
tetrabutyl ammonium fluoride; palladium in tetrahydrofuran T=70°C; Hiyama coupling; 1.5 h; Inert atmosphere;
参考文献
Srimani, Dipankar; Bej, Ansuman; Sarkar, Amitabha
Journal of Organic Chemistry, 2010 , vol. 75, # 12 p. 4296 - 4299
反应条件
titanium tetrachloride T=80°C; Alkylation; 48 h;
参考文献
Darbeau, Ron W.; White, Emu H.; Song, Fenhong; Darbeau, Nyla R.; Chou, James
Journal of Organic Chemistry, 1999 , vol. 64, # 16 p. 5966 - 5978
参考文献
Staedel
Justus Liebigs Annalen der Chemie, 1894 , vol. 283, p. 157
Full Text Show Details
Baeyer; Villiger
Chemische Berichte, 1904 , vol. 37, p. 605
反应条件
in dimethyl sulfoxide; nitrobenzene T=40°C; Rate constant;
参考文献
Doklady Chemistry, , vol. 266, p. 309 - 313
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 266, # 1 p. 131 - 134
反应条件
1: ethanol 2: platinum; ethanol / Hydrogenation 3: aqueous HBr View Scheme
参考文献
Burckhalter; Stephens
Journal of the American Chemical Society, 1951 , vol. 73, p. 56
反应条件
1: 6 h / Heating 2: 36N sulfuric acid / H2O / 0 °C View Scheme
参考文献
Brembilla, Alain; Roizard, Denis; Schoenleber, Jacqueline; Lochon, Pierre
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2330 - 2336
反应条件
hydrogenchloride; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane Multistep reaction;
参考文献
Hoefnagel, A. J.; Vos, R. H. de; Wepster, B. M.
Recueil des Travaux Chimiques des Pays-Bas, 1992 , vol. 111, # 1 p. 22 - 28