1-(氯甲基)-4-硝基苯合成路线 (共 349 条)
反应条件
potassium carbonate; sodium iodide
参考文献
Matsumoto
Chemical and pharmaceutical bulletin, 1967 , vol. 15, # 12 p. 1990 - 1995
反应条件
3 h; Ambient temperature;
参考文献
Bhattacharya, Pranab K.; Bandyopadhyay, Soumitra; Pakrashi, Satyesch
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 673 - 674
反应条件
N-benzyl-N,N,N-trimethyl-ammonium chloride; potassium carbonate in dichloromethane; water
T=20°C;
参考文献
Gorska, Agata; Chomicz, Lidia; Zebrowska, Justyna; Myjak, Przemyslaw; Augustynowicz-Kopec, Ewa; Zwolska, Zofia; Piekarczyk, Janusz; Rebandel, Henryk; Kazimierczuk, Zygmunt
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 1 p. 101 - 107
反应条件
in 1,4-dioxane; ruthenium
参考文献
Allied Chemical Corporation
Patent: US4024185 A1, 1977 ;
反应条件
potassium carbonate in dimethyl sulfoxide; acetonitrile
1.25 h; Irradiation;
参考文献
Gharbaoui, Tawfik; Benhida, Rachid; Chastanet, Jacqueline; Lechevallier, Andre; Maillos, Philippe; Beugelmans, Rene
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 561 - 574
反应条件
sodium hydroxide; Aliquatreg; 336 in hexane; water
10 h; Heating; Yield given. Yields of byproduct given;
参考文献
Shinkai, I.; Zwan, M. C. Vander; Hartner, F. W.; Reamer, R. A.; Tull, R. J.; Weinstock, L. M.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 197 - 198
反应条件
sodium hydride
1.) DMF, 30 deg C, 1 h, 2.) DMF, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rasmussen, Malcolm; Hope, Janet M.
Australian Journal of Chemistry, 1982 , vol. 35, # 3 p. 525 - 534
反应条件
potassium ethanolate
1.) EtOH, 2.) DMF, 30 deg C, 16 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rasmussen, Malcolm; Hope, Janet M.
Australian Journal of Chemistry, 1982 , vol. 35, # 3 p. 535 - 542
反应条件
1: ethanol
2: platinum; ethanol / Hydrogenation
View Scheme
参考文献
Burckhalter; Stephens
Journal of the American Chemical Society, 1951 , vol. 73, p. 56
反应条件
sulfur; triethylamine in dimethyl sulfoxide
T=20°C; 3 h;
参考文献
Thiel, W.; Mayer, R.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 2 p. 243 - 262