N,N-二甲基对硝基苯胺合成路线 (共 150 条)
反应条件
carbon monoxide; benzene; dodecacarbonyltetrarhodium(0) T=220°C; 6 h;
参考文献
Mise, Takaya; Hong, Pangbu; Yamazaki, Hiroshi
Chemistry Letters, 1980 , p. 439 - 440
反应条件
Ru/C; sodium hydroxide in tetrahydrofuran; ethanol T=80°C; 24 h; Microwave irradiation;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 13 p. 2412 - 2418
反应条件
Ru/C; sodium hydroxide in tetrahydrofuran; ethanol T=120°C; 24 h; Microwave irradiation;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 13 p. 2412 - 2418
参考文献
Weber
Chemische Berichte, 1877 , vol. 10, p. 761
反应条件
methanol; benzyltriphenylphosphonium tribromide; sodium hydrogencarbonate in dichloromethane 0.283333 h; Ambient temperature;
参考文献
Xin-teng, Ding; Guo-bin, Liu
Synthetic Communications, 1989 , vol. 19, # 7,8 p. 1261 - 1266
反应条件
ammonium cerium(IV) nitrate; sulfuric acid; urea 1.) MeOH, room temperature, 2.) 80 deg C, 20 h; Yield given. Multistep reaction;
参考文献
Galliani, Guido; Rindone, Bruno
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 828 - 832
反应条件
5,10,15,20-tetrakis-pentafluorophenyl-21H,23H-porphyrin iron(III) chloride; iodosylbenzene in dichloromethane 0.25 h; Ambient temperaturekinetic deuterium isotope effect (N-methyl-N-trideuteriomethyl- and N,N-bis(trideuteriomethylanilines); other N,N-dimethylanilines; Product distributionMechanism;
参考文献
Goto; Watanabe; Fukuzumi; Jones; Dinnocenzo
Journal of the American Chemical Society, 1998 , vol. 120, # 41 p. 10762 - 10763
反应条件
n-Butyl nitrite; ammonium chloride; water 2 h; Heating;
参考文献
Canadian Journal of Chemistry, , vol. 75, # 4 p. 469 - 473
反应条件
in dichloromethane Kinetics; mixing (223 K); not isolated; UV-VIS spectroscopy (413 nm);
参考文献
Goto; Watanabe; Fukuzumi; Jones; Dinnocenzo
Journal of the American Chemical Society, 1998 , vol. 120, # 41 p. 10762 - 10763
反应条件
ammonium cerium(IV) nitrate; sulfuric acid; urea 1.) AcOH, room temperature, 2.) 80 deg C, 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Galliani, Guido; Rindone, Bruno
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 828 - 832