1: 89 percent / diphenyl-2-pyridylphosphine; di-tert-butyl azodicarboxylate / CH2Cl2 / 2 h / 20 °C 2: 91 percent / PhSH; potassium carbonate / acetonitrile / 50 °C View Scheme
参考文献
Guisado, Cristina; Waterhouse, Jodie E.; Price, Wayne S.; Jorgensen, Michael R.; Miller, Andrew D.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 6 p. 1049 - 1057
1: iron; aqueous hydrochloric acid
2: aqueous HCl / 65 - 70 °C / Diazotization.Kochen des Reaktionsprodukts mit wss.-aethanol. KOH und mit Dimethylsulfat
View Scheme
参考文献
Bennett; Hafez
Journal of the Chemical Society, 1941 , p. 652,657