4,4'-二硝基二苯二硫醚合成路线 (共 219 条)
反应条件
1,10-phenanthroline; CuCl2·2H2O; tetrabutyl ammonium fluoride; caesium carbonate; sulfur in water T=100°C; 24 h; Sealed tube;
参考文献
Li, Zhengkai; Ke, Fang; Deng, Hang; Xu, Hualong; Xiang, Haifeng; Zhou, Xiangge
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 18 p. 2943 - 2946
反应条件
1: With potassium 5-methyl-1,3,4-oxadiazole-2-thiolate in N,N-dimethyl-formamide T=20°C; 0.333333 h; 2: With copper(l) chloride in N,N-dimethyl-formamide T=130°C; 7 h;
参考文献
Soleiman-Beigi, Mohammad; Mohammadi, Fariba
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7028 - 7030
反应条件
ziconium(IV) oxychloride octahydrate; sodium iodide in water T=90°C; 0.25 h;
参考文献
Jafarpour, Maasoumeh; Rezaeifard, Abdolreza; Heidari, Mahdieh
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 7 p. 1470 - 1482
反应条件
air in dimethyl sulfoxide T=80°C;
参考文献
Alam, Ashraful; Takaguchi, Yutaka; Tsuboi, Sadao
Synthetic Communications, 2005 , vol. 35, # 10 p. 1329 - 1333
反应条件
tetramethylstannane; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; 4 h;
参考文献
Cochran, John C.; Friedman, Susan R.; Frazier, John P.
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1533 - 1536
反应条件
1,10-phenanthroline; CuCl2·2H2O; tetrabutyl ammonium fluoride; caesium carbonate; sulfur in water T=100°C; 24 h; Sealed tube;
参考文献
Li, Zhengkai; Ke, Fang; Deng, Hang; Xu, Hualong; Xiang, Haifeng; Zhou, Xiangge
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 18 p. 2943 - 2946
反应条件
Na2S2 in 1-methyl-pyrrolidin-2-one
参考文献
Hoffmann; Polus; Hilczer; Goslar; Kiczka; Doczekalska
Polish Journal of Chemistry, 2003 , vol. 77, # 1 p. 87 - 98
反应条件
SeCl4 in ethylene glycol dimethyl ether T=0°C; 2 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 61, # 2 p. 441 - 445,401 - 404
反应条件
triphenylphosphine in benzene T=20°C; 1 h;
参考文献
Levchenko, E. S.; Dubinina, T. N.; Sereda, S. V.; Antipin, M. Yu.; Struchkov, Yu. T.; Boldeskul, I. E.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 75 - 81
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 1 p. 86 - 93
反应条件
hydrogen sulfide; tetraethylammonium hydroxide in methanol T=20°C; 0.5 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 9.2 p. 1901 - 1903
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 9 p. 2143 - 2145