4,4'-二硝基二苯二硫醚合成路线 (共 219 条)
反应条件
XeF2 in dichloromethane T=-20 - 5°C;
参考文献
Sipyagin; Enshov; Kashtanov; Potemkin; Thrasher; Waterfeld
Russian Chemical Bulletin, 2004 , vol. 53, # 2 p. 420 - 434
反应条件
CuO; potassium carbonate in N,N-dimethyl-formamide T=140°C; 48 h; Inert atmosphereSchlenk technique;
参考文献
Rosario, Alisson R.; Casola, Kamila K.; Oliveira, Carla E.S.; Zeni, Gilson
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 2960 - 2966
反应条件
magnesium in methanol 0.166667 h; Ambient temperature;
参考文献
Synthetic Communications, , vol. 27, # 8 p. 1347 - 1350
反应条件
sodium tetrahydroborate; zirconium tetrachloride in tetrahydrofuran T=35°C; Reduction; 0.166667 h;
参考文献
Synthetic Communications, , vol. 30, # 21 p. 3905 - 3911
参考文献
Chemische Berichte, , vol. 41, p. 2264
Justus Liebigs Annalen der Chemie, , vol. 400, p. 9
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide 0.25 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
dihydrogen peroxide; zirconium tetrachloride in water; acetonitrile T=25°C; 0.0166667 h;
参考文献
Veisi, Hojat; Sedrpoushan, Alireza; Hemmati, Saba; Kordestani, Davood
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 6 p. 769 - 775
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide 0.25 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
iodine in 1-methyl-pyrrolidin-2-one T=130°C; 0.666667 h; Sealed tubeMicrowave irradiation;
参考文献
Hu, Bolun; Sun, Leilei; Tang, Riyuan; Hu, Huanan
Chinese Journal of Chemistry, 2012 , vol. 30, # 10 p. 2556 - 2562,7
反应条件
sodium hydroxide; ethanol
参考文献
Fromm; Wittmann
Chemische Berichte, 1908 , vol. 41, p. 2264