4,4'-二硝基二苯二硫醚合成路线 （共 219 条）
反应条件
1: tetraethylammonium perchlorate / N,N-dimethyl-acetamide / electrochemical reduction (gold-grid electrode, cathodic and anodic compartments were separated by a sintered porous glass) 2: N,N-dimethyl-acetamide / 20 °C View Scheme
参考文献
Benaichouche, Meriem; Bosser, Gerard; Paris, Jacky; Plichon, Vincent
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 8 p. 1421 - 1424
反应条件
tetra-(n-butyl)ammonium iodide in benzene T=20°C; 5 h;
参考文献
Levchenko, E. S.; Dubinina, T. N.; Sereda, S. V.; Antipin, M. Yu.; Struchkov, Yu. T.; Boldeskul, I. E.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 75 - 81
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 1 p. 86 - 93
反应条件
tetra-(n-butyl)ammonium iodide in benzene T=20°C; 5 h;
参考文献
Levchenko, E. S.; Dubinina, T. N.; Sereda, S. V.; Antipin, M. Yu.; Struchkov, Yu. T.; Boldeskul, I. E.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 75 - 81
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 1 p. 86 - 93
参考文献
Journal of the Chemical Society, , p. 542
Zhurnal Obshchei Khimii, , vol. 2, p. 939,949, 950
Chem. Zentralbl., , vol. 105, # I p. 216
Journal of the Chemical Society, , p. 887,893
反应条件
(i) Cl2, (ii) /BRN= 956578/; Multistep reaction;
参考文献
Pilgram,K.; Korte,F.
Tetrahedron, 1965 , vol. 21, p. 1999 - 2013
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide 0.25 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide 0.25 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
1: chlorine 2: tetrachloromethane View Scheme
参考文献
Truitt et al.
Journal of the American Chemical Society, 1949 , vol. 71, p. 3511
反应条件
1: bis-(4-nitro-phenyl)-disulfide With tetrabutyl-ammonium chloride; water; chloramine-T in acetonitrile T=0°C; 0.5 h; 2: phenol With triethylamine in acetonitrile T=0 - 20°C; 1 h;
参考文献
Veisi, Hojat; Ataee, Meral; Fatolahi, Leila; Lotfi, Shahram
Letters in Organic Chemistry, 2013 , vol. 10, # 2 p. 111 - 117
反应条件
1: trichloroisocyanuric acid; tetrabutyl-ammonium chloride; water / acetonitrile / 0.5 h / 0 °C 2: triethylamine / acetonitrile / 1.5 h / 20 °C View Scheme
参考文献
Hemmati, Saba; Mojtahedi, Mohammad Majid; Abaee, Mohammad Saeed; Vafajoo, Zahra; Saremi, Shokufe Ghahri; Noroozi, Mohammad; Sedrpoushan, Alireza; Ataee, Meral
Journal of Sulfur Chemistry, 2013 , vol. 34, # 4 p. 347 - 357
