4,4'-二硝基二苯二硫醚合成路线 (共 219 条)
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
0.25 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
0.5 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
0.333333 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
sodium hydroxide; Thiourea sulfone; trimethylhexadecylammonium chloride in tetrahydrofuran; water
3.3 h; Heating;
参考文献
Comasseto, J. V.; Lang, E. S.; Ferreira, J. Tercio B.; Simonelli, F.; Correira, V. R.
Journal of Organometallic Chemistry, 1987 , vol. 334, p. 329 - 340
反应条件
copper(l) iodide; oxygen in N,N-dimethyl-formamide
T=120°C; 24 h;
参考文献
Zhang, Shouhui; Qian, Pengcheng; Zhang, Manli; Hu, Maolin; Cheng, Jiang
Journal of Organic Chemistry, 2010 , vol. 75, # 19 p. 6732 - 6735
反应条件
potassium hydroxide in tert-butyl alcohol
T=30°C; Rate constant;
参考文献
Happer,D.A.R. et al.
Australian Journal of Chemistry, 1973 , vol. 26, p. 121 - 134
参考文献
Levchenko, E. S.; Dubinina, T. N.; Budnik, L. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 10 p. 1875 - 1880
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 10 p. 2158 - 2163
反应条件
chlorine in tetrachloromethane
T=60°C; 3 h;
参考文献
Johnston,M.; Raines,R.; Walsh,C.
Journal of the American Chemical Society, 1980 , vol. 102, p. 4241
反应条件
tetrabutyl-ammonium chloride in benzene
1.) reflux, 15 min, 2.) 20 deg C, 4 h;
参考文献
Levchenko, E. S.; Dubinina, T. N.; Budnik, L. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 10 p. 1875 - 1880
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 10 p. 2158 - 2163
反应条件
unter Ausschluss der Luftfeuchtigkeit;
参考文献
Zincke; Lenhardt
Justus Liebigs Annalen der Chemie, 1913 , vol. 400, p. 9