in melt
stirring of 7.37 mmol triphenyltin hydride and 11 mmol 4-vinylpyridine at 100°C for 0.5 h as a melt under N2;; recrystallization from petroleum ether yields hexaphenylditin; evaporation of the mother liquor to dryness under reduced pressure; recrystallization from petroleum ether; elem. anal.;;
参考文献
Mahon, Mary F.; Molloy, Kieran C.; Waterfield, Philip C.
Organometallics, 1993 , vol. 12, p. 769 - 774
bis(acetylacetonate)nickel(II); triethylaluminum; triphenylphosphine in toluene
T=150°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Selimov, F. A.; Ptashko, O. A.; Fatykhov, A. A.; Khalikova, N. R.; Dzhemilev, U. M.
Russian Chemical Bulletin, 1993 , vol. 42, # 5 p. 872 - 878
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 5 p. 916 - 921
