1: With chloro-trimethyl-silane; mischmetal in tetrahydrofuran 3 h; Inert atmosphereReflux; 2: With water in tetrahydrofuran 0.0833333 h; Alkaline conditions;
参考文献
Vellemaee, Eerold; Stepanov, Vladimir; Maeorg, Uno
Synthetic Communications, 2010 , vol. 40, # 22 p. 3397 - 3404
1: dimethylamine borane With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2: para-chloro-benzonitrile in tetrahydrofuran; hexane T=65°C; 12 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 66, # 6 p. 1999 - 2004
1: dimethylamine borane With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2: para-bromobenzonitrile in tetrahydrofuran; hexane T=65°C; 12 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 66, # 6 p. 1999 - 2004
