1: 4-methoxy-benzoic acid With N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide
T=0°C; 0.166667 h;
2: benzylamine in N,N-dimethyl-formamide
T=20°C; 0.916667 h; Further stages.;
4 A molecular sieve; phenolated sodium; palladium diacetate in dimethyl sulfoxide
T=110°C; P=760.051 Torr; 15 h;
参考文献
Martinelli, Joseph R.; Clark, Thomas P.; Watson, Donald A.; Munday, Rachel H.; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 44 p. 8460 - 8463
