反应条件
1: 97.8 percent / p-toluenesulfonic acid monohydrate / toluene / 3 h / Heating
2: 0.87 g / nitromethane / 66 h / 20 °C
3: 57.2 percent / tetrabutylammonium bromide; aq. NaOH / 0.5 h / Heating
4: 63 percent / LiAlH4 / tetrahydrofuran / 17 h / 20 °C
5: 72.5 percent / BF3*OEt2 / CH2Cl2 / 1 h / 0 °C
View Scheme
参考文献
Maguire, Anita R.; Plunkett, Stephen J.; Papot, Sebastien; Clynes, Martin; O'Connor, Robert; Touhey, Samantha
Bioorganic and Medicinal Chemistry, 2001 , vol. 9, # 3 p. 745 - 762