1: benzylamine With sodium hydride in tetrahydrofuran; mineral oil T=20°C; 0.0333333 h; Inert atmosphere; 2: alpha-chloromethyl-naphthalene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; mineral oil T=20°C; 17 h; Inert atmosphere; regioselective reaction;
参考文献
Zhang, Sheng; Wang, Yi; Feng, Xiujuan; Bao, Ming
Journal of the American Chemical Society, 2012 , vol. 134, # 12 p. 5492 - 5495
Armesto, Diego; Ortiz, Maria J.; Perez-Ossorio, Rafael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 2021 - 2026
1: benzylamine With hydrogenchloride in tetrahydrofuran 2: cyanoguanidine hydrochloride T=20 - 140°C;
参考文献
Gravestock, David; Rousseau, Amanda L.; Lourens, Anna C.U.; Moleele, Simon S.; Van Zyl, Robyn L.; Steenkamp, Paul A.
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 6 p. 2022 - 2030
1: aq.-ethanolic NaHCO3 / anschliessendes Behandeln mit Chlorokohlensaeure-aethylester und Erhitzen des Reaktionsprodukts mit HN3 in Benzol 2: aqueous KOH View Scheme
参考文献
Garbrecht; Herbst
Journal of Organic Chemistry, 1953 , vol. 18, p. 1003,1005