Pinner; Klein
Chemische Berichte, 1878 , vol. 11, p. 764
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Gumpert
Journal fuer Praktische Chemie (Leipzig), 1884 , vol. <2> 30, p. 88
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Pinner
Die Imidoaether und ihre Derivate <Berlin 1892>, S. 166
in tetrahydrofuran conventional Schlenk technique; PhCN added with stirring to NdI2; 5 min;PhCN removed in vac.; THF added; pptd. for 1 h; decanted; solvent remov ed from mother liquor; MeOH added; pptd. (20°C, 20 h); MeOH removed from soln.; pptd. by adding H2O; ppt. after decantation washed with cold THF, dried in vac. (NdI3(thf)3);ppt. after H2O addition sepd. by centrifuging, dried (NdI(OH)2(H2O)5); elem. anal.;
参考文献
Balashova; Khoroshenkov; Kusyaev; Eremenko; Aleksandrov; Fukin; Bochkarev
Russian Chemical Bulletin, 2004 , vol. 53, # 4 p. 825 - 829