tert.-butylhydroperoxide; trifluoroacetic acid in dichloromethane; water T=23°C; 24 h; regioselective reaction;
参考文献
Fujiwara, Yuta; Dixon, Janice A.; Rodriguez, Rodrigo A.; Baxter, Ryan D.; Dixon, Darryl D.; Collins, Michael R.; Blackmond, Donna G.; Baran, Phil S.
Journal of the American Chemical Society, 2012 , vol. 134, # 3 p. 1494 - 1497
Richter, Isabella; Minari, Jusaku; Axe, Philip; Lowe, John P.; James, Tony D.; Sakurai, Kazuo; Bull, Steven D.; Fossey, John S.
Chemical Communications, 2008 , # 9 p. 1082 - 1084
1: diethylamine With n-butyllithium in tetrahydrofuran; hexane
T=0 - 20°C; 0.25 h;
2: 4-pyridinecarbonitrile With cesium fluoride in tetrahydrofuran; hexane
T=65°C; 2 h; Further stages.;
参考文献
Penney, Jonathan M.
Tetrahedron Letters, 2004 , vol. 45, # 12 p. 2667 - 2669
