1: benzyl alcohol With sodium hydride in tetrahydrofuran; mineral oil T=0°C; 0.25 h; Inert atmosphere; 2: 3-fluoro-4-nitro-benzoic acid in tetrahydrofuran; mineral oil T=0 - 25°C; 2.08333 h; Inert atmosphere;
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15-crown-5; sodium hydroxide in toluene 4 h; Dean-StarkReflux;
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