反应条件
1: α-(2,4-difluorophenyl)-α-(1H-1,2,4-triazol-1-ylmethyl)-1H-1,2,4-triazol-1-ethanol With pyridine; phosphorus trichoride in dichloromethane T=-13 - 13°C; 2.08333 h; Inert atmosphereIndustrial scale; 2: benzyl alcohol in dichloromethane T=10 - 16°C; 4 h; Inert atmosphereIndustrial scale; 3: With dihydrogen peroxide in dichloromethane; water T=0 - 20°C; 4 h; Industrial scale;
参考文献
Bentley, Arthur; Butters, Michael; Green, Stuart P.; Learmonth, William J.; MacRae, Julie A.; Morland, Matthew C.; O'Connor, Garry; Skuse, Joanne
Organic Process Research and Development, 2002 , vol. 6, # 2 p. 109 - 112
