反应条件
1: 1) sodium hydroxide (2 M); 2) sodium borohydride / 1) 30 min; 2) 6-10 deg C, 1+1+1+2 h 2: 28 percent / sodium hydroxide / H2O / 0 deg C, 30 min, 30-33 deg C, 2 h 3: 1) borane-dimethylsulphide complex, triethylamine; 2) aq. sodium hydroxide (2M) / 1) THF, 0 deg C, 15 min; 2) reflux, 6 h View Scheme
参考文献
Brown, George R.; Foubister, Alan J.; Wright, Brian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2577 - 2580