反应条件
1: 1-iodo-tridecafluoro-hexane; n-butyl-magnesium chloride With bis(cyclopentadienyl)titanium dichloride in 1,4-dioxane; diethyl ether T=-78 - -50°C; 2 h; Inert atmosphere; 2: benzaldehyde in 1,4-dioxane; diethyl ether T=20°C; 2 h; Inert atmosphere;
参考文献
Fujiu, Motohiro; Hashimoto, Ryota; Nakamura, Yuzo; Aikawa, Kohsuke; Ito, Shigekazu; Mikami, Koichi
Chemistry - A European Journal, 2014 , vol. 20, # 8 p. 2382 - 2386