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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苄硫醇
合成路线
（共 1080 条）
82737-35-7
+
100-53-8
苄硫醇
→
反应条件
32812-87-6
反应条件
in benzene at room temp. for 48 h, PbPh2cp2:PhCH2SH=1:2, under Ar in the dark; alem. anal.;
参考文献
Gaffney, Christine; Harrison, Philip G.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1982 , p. 1055 - 1060
141-79-7
异丙叉丙酮
+
100-53-8
苄硫醇
→
反应条件
19361-06-9
反应条件
bis-(trifluoromethylsulphonyl)amine in dichloromethane T=20°C; Michael addition; 0.166667 h;
参考文献
Wabnitz, Tobias C.; Spencer, Jonathan B.
Organic Letters, 2003 , vol. 5, # 12 p. 2141 - 2144
1567-73-3
+
100-53-8
苄硫醇
+
67-64-1
丙酮
→
反应条件
19361-06-9
反应条件
1: acetone With 6'-hydroxy-9-amino-9-deoxy-epiquinidine; (S)-BINOL-phosphoric acid T=20°C; 0.166667 h; 2: (E)-3-methylpent-3-en-2-one; phenylmethanethiol T=40°C; sulfa Michael addition; 60 h; optical yield given as percent destereoselective reaction;
参考文献
Tian, Xu; Cassani, Carlo; Liu, Yankai; Moran, Antonio; Urakawa, Atsushi; Galzerano, Patrizia; Arceo, Elena; Melchiorre, Paolo
Journal of the American Chemical Society, 2011 , vol. 133, # 44 p. 17934 - 17941
1567-73-3
+
100-53-8
苄硫醇
+
67-64-1
丙酮
→
反应条件
19361-06-9
反应条件
1: acetone With C19H23N3O; (S)-BINOL-phosphoric acid T=20°C; 0.166667 h; 2: (E)-3-methylpent-3-en-2-one; phenylmethanethiol T=40°C; sulfa Michael addition; 60 h; optical yield given as percent destereoselective reaction;
参考文献
Tian, Xu; Cassani, Carlo; Liu, Yankai; Moran, Antonio; Urakawa, Atsushi; Galzerano, Patrizia; Arceo, Elena; Melchiorre, Paolo
Journal of the American Chemical Society, 2011 , vol. 133, # 44 p. 17934 - 17941
107368-26-3
+
100-53-8
苄硫醇
+
67-64-1
丙酮
→
反应条件
19361-06-9
反应条件
1: acetone With 6'-hydroxy-9-amino-9-deoxy-epiquinidine; (S)-BINOL-phosphoric acid T=20°C; 0.166667 h; 2: (E)-Ethyl 3-methyl-4-oxo-2-pentenoate; phenylmethanethiol T=40°C; sulfa Michael addition; 60 h; optical yield given as percent eestereoselective reaction;
参考文献
Tian, Xu; Cassani, Carlo; Liu, Yankai; Moran, Antonio; Urakawa, Atsushi; Galzerano, Patrizia; Arceo, Elena; Melchiorre, Paolo
Journal of the American Chemical Society, 2011 , vol. 133, # 44 p. 17934 - 17941
→
反应条件
19361-06-9
反应条件
1: acetone With 6'-hydroxy-9-amino-9-deoxy-epiquinidine; (S)-BINOL-phosphoric acid T=20°C; 0.166667 h; 2: (E)-3-methyl-4-(4-methoxyphenyl)-3-buten-2-one; phenylmethanethiol T=40°C; sulfa Michael addition; 60 h; optical yield given as percent eestereoselective reaction;
参考文献
Tian, Xu; Cassani, Carlo; Liu, Yankai; Moran, Antonio; Urakawa, Atsushi; Galzerano, Patrizia; Arceo, Elena; Melchiorre, Paolo
Journal of the American Chemical Society, 2011 , vol. 133, # 44 p. 17934 - 17941
→
反应条件
19361-06-9
反应条件
1: acetone With 6'-hydroxy-9-amino-9-deoxy-epiquinidine; (S)-BINOL-phosphoric acid T=20°C; 0.166667 h; 2: 3-[1-(4-Nitro-phenyl)-meth-(E)-ylidene]-pentan-2-one; phenylmethanethiol T=40°C; sulfa Michael addition; 60 h; optical yield given as percent eestereoselective reaction;
参考文献
Tian, Xu; Cassani, Carlo; Liu, Yankai; Moran, Antonio; Urakawa, Atsushi; Galzerano, Patrizia; Arceo, Elena; Melchiorre, Paolo
Journal of the American Chemical Society, 2011 , vol. 133, # 44 p. 17934 - 17941
35044-52-1
+
100-53-8
苄硫醇
→
反应条件
19361-06-9
反应条件
Behandlung des Reaktionsprodukts mit wss. HCl;
参考文献
Banerjee; Chakraborty; Dutta
Science and Culture, 1949 , vol. 14, p. 438
13037-60-0
2-溴苯基异硫氰酸酯
+
100-53-8
苄硫醇
→
反应条件
19654-17-2
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium carbonate in 1,4-dioxane T=90°C; 16 h;
参考文献
Murru, Siva; Mondal, Pravat; Yella, Ramesh; Patel, Bhisma K.
European Journal of Organic Chemistry, 2009 , # 31 p. 5406 - 5413
75-15-0
+
615-43-0
+
100-53-8
苄硫醇
→
反应条件
19654-17-2
反应条件
1: carbon disulfide; phenylmethanethiol With caesium carbonate in N,N-dimethyl-formamide T=20°C; 1 h; 2: 2-iodo aniline With copper(I) bromide in N,N-dimethyl-formamide T=110°C; 12 h;
参考文献
Shi, Liu; Liu, Xiangqian; Zhang, Hui; Jiang, Yongwen; Ma, Dawei
Journal of Organic Chemistry, 2011 , vol. 76, # 10 p. 4200 - 4204
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