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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苄硫醇
合成路线
（共 1080 条）
→
反应条件
4786-75-8
反应条件
potassium tert-butylate in tetrahydrofuran; isopropyl alcohol T=85°C; 48 h;
参考文献
Millennium Pharmaceuticals, Inc.
Patent: US2007/191293 A1, 2007 ;
Location in patent: Page/Page column 53 ;
4526-07-2
1,4-双(三甲硅基)-1,3-丁二炔
+
100-53-8
苄硫醇
→
反应条件
反应条件
Yield givenMultistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Block, Eric; Birringer, Marc; He, Chunhong
Angewandte Chemie - International Edition, 1999 , vol. 38, # 11 p. 1604 - 1607
4526-07-2
1,4-双(三甲硅基)-1,3-丁二炔
+
1482-82-2
二苄基二硒醚
+
100-53-8
苄硫醇
→
反应条件
反应条件
Yield givenMultistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Block, Eric; Birringer, Marc; He, Chunhong
Angewandte Chemie - International Edition, 1999 , vol. 38, # 11 p. 1604 - 1607
3709-08-8
Alpha,Alpha-二甲基-γ-丁内酯
+
100-53-8
苄硫醇
→
反应条件
499194-48-8
反应条件
sodium hydride in toluene Heating;
参考文献
Vrudhula, Vivekananda M; MacMaster, John F; Li, Zhengong; Kerr, David E; Senter, Peter D
Bioorganic and medicinal chemistry letters, 2002 , vol. 12, # 24 p. 3591 - 3594
624-31-7
4-碘甲苯
+
100-53-8
苄硫醇
→
反应条件
5023-60-9
反应条件
tetra(n-butyl)ammonium hydroxide in water T=50°C; 24 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Xu, Hua-Jian; Liang, Yu-Feng; Zhou, Xin-Feng; Feng, Yi-Si
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 13 p. 2562 - 2568
106-38-7
对溴甲苯
+
100-53-8
苄硫醇
→
反应条件
5023-60-9
反应条件
1: phenylmethanethiol With sodium t-butanolate in tetrahydrofuran T=23°C; 0.166667 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran 0.166667 h; Inert atmosphere; 3: para-bromotoluene With [P(t-Bu)3Pd(μ-Br)]2; lithium iodide in tetrahydrofuran T=90°C; 2 h; Inert atmosphere;
参考文献
Bastug, Gulluzar; Nolan, Steven P.
Journal of Organic Chemistry, 2013 , vol. 78, # 18 p. 9303 - 9308
106-43-4
对氯甲苯
+
100-53-8
苄硫醇
→
反应条件
5023-60-9
反应条件
(SIPr)Pd(Py)Cl2; potassium tert-butylate in toluene T=100°C; 20 h; Inert atmosphere;
参考文献
Shi, Yanhui; Cai, Zhengyuan; Guan, Pei; Pang, Guangsheng
Synlett, 2011 , # 14 art. no. W09311ST, p. 2090 - 2096
100-53-8
苄硫醇
→
反应条件
5023-60-9
反应条件
1: 52 percent / tetrahydrofuran / 1 h / 0 °C 2: 85 percent / KHCO3; (Bu4N)I / Pd(OAc)2; PPh3 / dioxane / 19 h / 100 °C View Scheme
参考文献
Harayama, Hiroto; Nagahama, Takayuki; Kozera, Toyohiro; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 445 - 456
90-11-9
1-溴代萘
+
100-53-8
苄硫醇
→
反应条件
5023-64-3
反应条件
1: phenylmethanethiol With sodium t-butanolate in tetrahydrofuran T=23°C; 0.166667 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran 0.166667 h; Inert atmosphere; 3: 1-Bromonaphthalene With [P(t-Bu)3Pd(μ-Br)]2; lithium iodide in tetrahydrofuran T=90°C; 2 h; Inert atmosphere;
参考文献
Eichman, Chad C.; Stambuli, James P.
Journal of Organic Chemistry, 2009 , vol. 74, # 10 p. 4005 - 4008
90-14-2
1-碘萘
+
100-53-8
苄硫醇
→
反应条件
5023-64-3
反应条件
tetra(n-butyl)ammonium hydroxide in water T=50°C; 24 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Xu, Hua-Jian; Liang, Yu-Feng; Zhou, Xin-Feng; Feng, Yi-Si
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 13 p. 2562 - 2568
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