1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexane
T=0°C;
2: With zinc dibromide in tetrahydrofuran; hexane
T=0°C;
3: pyridine-3-carbonitrile With n-tridecane; [NiCl2(PMe3)2] in tetrahydrofuran
T=65°C; 20 h; Further stages.;
参考文献
Penney, Jonathan M.; Miller, Joseph A.
Tetrahedron Letters, 2004 , vol. 45, # 25 p. 4989 - 4992
1: furan With n-butyllithium in diethyl ether
2 h; Heating;
2: pyridine-3-carbonitrile in diethyl ether
T=-78 - 20°C;
3: With hydrogenchloride in diethyl ether
参考文献
Chubb; Bryce; Tarbit
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 16 p. 1853 - 1854
