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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
溴化苯基镁
合成路线
（共 1496 条）
100-58-3
溴化苯基镁
+
88-05-1
2,4,6-三甲基苯胺
→
反应条件
92-52-4
联苯
+
23592-67-8
2,4,6-三甲基-N-苯基苯胺
反应条件
1: 2,4,6-trimethylbenzenamine With n-butyllithium; ZnCl2*TMEDA in tetrahydrofuran; hexane T=0 - 20°C; 0.5 h; Inert atmosphereSchlenk technique; 2: phenyl-magnesium bromide With N,N'-dimethyl-N,N'-propyleneurea; bis(acetylacetonate)nickel(II); 1,2-dichloro-2-methylpropane in tetrahydrofuran; hexane T=0 - 20°C; 3 h; Inert atmosphereSchlenk technique;
参考文献
Ilies, Laurean; Matsubara, Tatsuaki; Nakamura, Eiichi
Organic Letters, 2012 , vol. 14, # 21 p. 5570 - 5573,4
612-55-5
2-碘萘
+
100-58-3
溴化苯基镁
→
反应条件
591-50-4
碘苯
+
2430-34-4
反应条件
1: in tetrahydrofuran; toluene T=60°C; 24 h; Inert atmosphere; 2: With water-d2 in tetrahydrofuran
参考文献
Shirakawa, Eiji; Hayashi, Yumi; Itoh, Ken-Ichi; Watabe, Ryo; Uchiyama, Nanase; Konagaya, Wataru; Masui, Seiji; Hayashi, Tamio
Angewandte Chemie - International Edition, 2012 , vol. 51, # 1 p. 218 - 221
100-58-3
溴化苯基镁
→
反应条件
13962-92-0
反应条件
1: 89 percent / PdCl2(dppb) / tetrahydrofuran / 16 h / Heating 2: 66 percent / aq. KMnO4 / pyridine View Scheme
参考文献
Kelley, Charles J.; Ghiorghis, Alem; Kauffman, Joel M.
Journal of Chemical Research, Miniprint, 1997 , # 12 p. 2701 - 2733
31161-46-3
+
100-58-3
溴化苯基镁
→
反应条件
92-52-4
联苯
+
13858-68-9
反应条件
1: phenyl-magnesium bromide With bismuth(III) chloride 2: 2-benzoyl-5-bromothiophene With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
130339-76-3
+
100-58-3
溴化苯基镁
→
反应条件
92-52-4
联苯
+
13858-68-9
反应条件
1: phenyl-magnesium bromide With bismuth(III) chloride 2: (5-iodo-2-thienyl)(phenyl)methanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
→
反应条件
134746-11-5
反应条件
in diethyl ether; toluene T=-20 - 0°C; Beckmann Rearrangement; 1.5 h; Inert atmosphere;
参考文献
Kang, Zhi-Yun; Zhang, Qing-Jian; Chen, Ruo-Yun; Zhang, Pei-Cheng; Yu, De-Quan
Journal of Asian Natural Products Research, 2013 , vol. 15, # 8 p. 840 - 848
22037-28-1
+
100-58-3
溴化苯基镁
→
反应条件
13679-41-9
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in diethyl ether 16 h; Ambient temperature;
参考文献
Pridgen, Lendon N.; Jones, Stella S.
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1590 - 1592
100-58-3
溴化苯基镁
→
反应条件
141190-94-5
反应条件
1: 77 percent / ZnBr2 / diethyl ether 2: 100 percent / pyridine / CH2Cl2 / Ambient temperature 3: p-toluenesulfonic acid monohydrate / methanol / 4 h / Heating 4: 1.) NaIO4, aq. NaHCO3, 2.) NaClO2, NaH2PO4 / 1.) CH2Cl2, room temp., 2 h, 2.) CH3CN, H2O, 10 deg C, 2 h 5: diethyl ether 6: 96 percent / H2 / Pd(OH)2/C / methanol View Scheme
参考文献
Merino, Pedro; Castillo, Elena; Franco, Santiago; Merchan, Francisco L.; Tejero, Tomas
Journal of Organic Chemistry, 1998 , vol. 63, # 7 p. 2371 - 2374
100-58-3
溴化苯基镁
→
反应条件
1530-11-6
反应条件
1.1: diethyl ether / -78 - 20 °C 2.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 8 h / 0 - 60 °C 3.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C 3.2: 20 °C 4.1: diethyl ether; hexane / -78 - 20 °C 5.1: chloro-trimethyl-silane / dichloromethane / 2 h / 20 °C View Scheme
参考文献
Too, Pei Chui; Tnay, Ya Lin; Chiba, Shunsuke
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1217 - 1225
2058-74-4
+
100-58-3
溴化苯基镁
→
反应条件
15757-32-1
反应条件
in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
Piemontesi, Cyril; Wang, Qian; Zhu, Jieping
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 9 p. 1533 - 1536
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