1: phenyl-magnesium bromide With ZnCl2*TMEDA in tetrahydrofuran
T=0°C; Inert atmosphere;
2: N-(4-methoxy-phenyl)-(1-phenyl-ethylidene)-amine With iron (III) acetylacetonate; 1,2-dichloro-2-methylpropane; 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran
T=0°C; 20 h; Inert atmosphere;
3: With hydrogenchloride; water in tetrahydrofuran
T=20°C; 3 h; chemoselective reaction;
1: phenyl-magnesium bromide With ZnCl2*TMEDA in tetrahydrofuran
T=0°C; Inert atmosphere;
2: N-(1-(4-bromophenyl)ethylidene)-4-methoxybenzenamine With iron (III) acetylacetonate; 1,2-dichloro-2-methylpropane; 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran
T=0°C; 20 h; Inert atmosphere;
3: With hydrogenchloride; water in tetrahydrofuran
T=20°C; 3 h;
1: phenyl-magnesium bromide With ZnCl2*TMEDA in tetrahydrofuran
T=0°C; Inert atmosphere;
2: N-(1-(4-bromophenyl)ethylidene)-4-methoxybenzenamine With iron (III) acetylacetonate; 1,2-dichloro-2-methylpropane; 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran
T=0°C; 48 h; Inert atmosphere;
3: With hydrogenchloride; water in tetrahydrofuran
T=20°C; 3 h; chemoselective reaction;
1: phenyl-magnesium bromide With ZnCl2*TMEDA in tetrahydrofuran
T=0°C; Inert atmosphere;
2: N-(1-(4-iodophenyl)ethylidene)-4-methoxybenzenamine With iron (III) acetylacetonate; 1,2-dichloro-2-methylpropane; 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran
T=0°C; 3 h; Inert atmosphere;
3: With hydrogenchloride; water in tetrahydrofuran
T=20°C; 3 h; chemoselective reaction;
Misra, B. K.; Rao, Y. R.; Mahapatra, S. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 10 p. 908 - 911
Misra, B. K.; Rao, Y. R.; Mahapatra, S. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 10 p. 908 - 911
Misra, B. K.; Rao, Y. R.; Mahapatra, S. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 10 p. 908 - 911