1: phenyl-magnesium bromide With ZnI2(tmeda) in tetrahydrofuran
2: (4'-Oxapentan-2'-yl) toluene-p-sulfonate With anhydrous iron chloride in tetrahydrofuran
T=0 - 40°C;
copper(l) iodide in tetrahydrofuran; toluene
T=-78 - 20°C; 16 h;
参考文献
Smith, Sean M.; Hoang, Gia L.; Pal, Rhitankar; Khaled, Mohammad O. Bani; Pelter, Liberty S. W.; Zeng, Xiao Cheng; Takacs, James M.
Chemical Communications, 2012 , vol. 48, # 100 p. 12180 - 12182