1: 3 mol percent NiCl2(Ph2PCH2CH2PPh2) / diethyl ether / 1 h / Ambient temperature 2: NiCl2(Ph2PCH2CH2PPh2) / diethyl ether / 8 h / Ambient temperature; var. time View Scheme
参考文献
Fiandanese, Vito; Marchese, Giuseppe; Naso, Francesco; Ronzini, Ludovico
Journal of the Chemical Society, Chemical Communications, 1982 , # 12 p. 647 - 649
1: in tetrahydrofuran T=0 - 20°C; 1 h; 2: With FeCl2(TMS-SciOPP) in tetrahydrofuran T=80°C; 12 h; 3: With hydrogenchloride in tetrahydrofuran; water T=0 - 20°C; 3 h;
参考文献
Chemical Communications, , vol. 48, # 75 p. 9376 - 9378