in tetrahydrofuran soln. of Mg compd. in THF was added dropwise to stirred cold suspn. of Co complex in THF under N2; stirred for 2 h; refluxed for 0.5 h; quenched with cold aq. HCl; filtered; petroleum ether added; filtered; residue combined; washed (EtOH, petroleum ether, H2O); dried (vac., P2O5); chromd. (silica gel, 20percent EtOAc/CHCl3); elem. anal.;
参考文献
Kumar, Kamlesh; Gupta
Journal of Organometallic Chemistry, 2010 , vol. 695, # 19-20 p. 2233 - 2239
