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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
溴化苯基镁
合成路线
（共 1496 条）
→
反应条件
37778-99-7
(S)-2-苯基-1-丙醇
+
1123-85-9
2-苯基-1-丙醇
反应条件
1: phenyl-magnesium bromide With copper(I) bromide dimethylsulfide complex in tetrahydrofuran Cooling with ice; 2: (Z)-1-phenylhex-4-en-3-yl pyridine-2-carboxylate in tetrahydrofuran T=-60 - -40°C; optical yield given as percent eeFurther stages;
参考文献
Kiyotsuka, Yohei; Acharya, Hukum P.; Katayama, Yuji; Hyodo, Tomonori; Kobayashi, Yuichi
Organic Letters, 2008 , vol. 10, # 9 p. 1719 - 1722
392-56-3
六氟苯
+
100-58-3
溴化苯基镁
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
反应条件
tris-(dibenzylideneacetone)dipalladium(0); [Pd(P{(C6H11)3})2]; lithium iodide in tetrahydrofuran T=60°C; 6 h; Inert atmosphereGlovebox; Reagent/catalystTime;
参考文献
Ohashi, Masato; Doi, Ryohei; Ogoshi, Sensuke
Chemistry - A European Journal, 2014 , vol. 20, # 7 p. 2040 - 2048
100-58-3
溴化苯基镁
→
反应条件
289656-45-7
反应条件
1.1: toluene; tetrahydrofuran / 20 - 50 °C / |Large scale 2.1: indium(III) chloride / toluene / 0.5 h / 20 °C / |Large scale 2.2: 2.5 h / 20 - 40 °C / |Large scale 3.1: potassium hydroxide / 1,1-dimethylpropan-1-ol / 10.5 h / 85 - 95 °C / |Large scale View Scheme
参考文献
Organic Process Research and Development, , vol. 16, # 8 p. 1385 - 1392
100-58-3
溴化苯基镁
→
反应条件
289656-45-7
+
386-95-8
反应条件
1.1: toluene; tetrahydrofuran / 20 - 50 °C / |Large scale 2.1: indium(III) chloride / toluene / 0.5 h / 20 °C / |Large scale 2.2: 2.5 h / 20 - 40 °C / |Large scale 3.1: potassium hydroxide / 1,1-dimethylpropan-1-ol / 12 h / 100 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 16, # 8 p. 1385 - 1392
100-58-3
溴化苯基镁
→
反应条件
289656-45-7
+
386-95-8
+
1391151-86-2
反应条件
1.1: toluene; tetrahydrofuran / 20 - 50 °C / |Large scale 2.1: indium(III) chloride / toluene / 0.5 h / 20 °C / |Large scale 2.2: 2.5 h / 20 - 40 °C / |Large scale 3.1: sulfuric acid; acetic acid / 125 - 130 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 16, # 8 p. 1385 - 1392
100-58-3
溴化苯基镁
+
107-02-8
→
反应条件
21087-29-6
反应条件
1: in tetrahydrofuran T=0°C; 2: With niobium pentachloride in tetrahydrofuran; 1,4-dioxane Inert atmosphere;
参考文献
Ravikumar; Yao, Lihua; Fleming, Fraser F.
Journal of Organic Chemistry, 2009 , vol. 74, # 19 p. 7294 - 7299
13187-99-0
+
100-58-3
溴化苯基镁
→
反应条件
112-40-3
+
112-41-4
+
1652-96-6
+
2719-61-1
反应条件
1: phenyl-magnesium bromide With vanadium(III) chloride in tetrahydrofuran T=20°C; 0.333333 h; 2: 2-bromododecane in tetrahydrofuran T=25°C; 1 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 81, # 2 p. 287 - 290
78-10-4
+
100-58-3
溴化苯基镁
→
反应条件
780-69-8
反应条件
in tetrahydrofuran
参考文献
Cheong, Hyeonsook; Roh, Sung-Hee; Cho, Myong-Shik; Kim, Myoung-Hee; Woo, Hee-Gweon; Yang, Kap-Seung; Kim, Bo-Hye; Jun, Jin; Sohn, Honglae
Journal of Nanoscience and Nanotechnology, 2013 , vol. 13, # 1 p. 702 - 705
100-58-3
溴化苯基镁
→
反应条件
119-62-0
反应条件
1: 1.) (COCl)2, DMSO, i-Pr2NEt / 1.) CH2Cl2, -78 deg C, 2.) THF, room temp. 2: Bu4NF / tetrahydrofuran / 0 - 25 °C 3: DMAP / pyridine 4: F3CCO2H / 0 °C 5: DMAP / pyridine 6: conc. HNO3, conc. H2SO4 / -20 - 25 °C 7: aq. HCl / 90 °C View Scheme
参考文献
Veeresa; Datta, Apurba
Tetrahedron Letters, 1998 , vol. 39, # 46 p. 8503 - 8004
21948-75-4
+
100-58-3
溴化苯基镁
→
反应条件
1008-89-5
+
366-18-7
+
100-68-5
+
1193-82-4
反应条件
in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 34, p. 123 - 132
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