反应条件
sulfuric acid in tetrahydrofuran; diethyl ether C6H5MgBr in ether was added dropwise to a soln. of (CH3)3CC6H3O2SbCl in anhydrous THF (argon atmosphere), stirring at -70°C for 2.5h, addition of 6M H2SO4, heating at 60°C for 1h; VPC-analysis;
参考文献
McEwen, William E.; Tien, J.-H.; Rembetsy, L. M.; Kalbacher, B. J.; Lubinkowski, Jacek J.; et al.
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 36, p. 153 - 164
