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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯基氯化镁
合成路线
（共 514 条）
29540-83-8
对苄基三氟甲磺酸
+
100-59-4
苯基氯化镁
→
反应条件
613-33-2
4,4'-二甲基联苯
+
644-08-6
4-甲基联苯
反应条件
2-phenyl-1H-imidazole; nickel dichloride in tetrahydrofuran T=50 - 60°C; Kumada Cross-Coupling; 3 h; Inert atmosphereSchlenk technique;
参考文献
Heterocycles, , vol. 86, # 1 p. 713 - 718
106-38-7
对溴甲苯
+
100-59-4
苯基氯化镁
→
反应条件
92-52-4
联苯
+
644-08-6
4-甲基联苯
反应条件
bis(carbene)-derived nickel(II)-pincer complex in tetrahydrofuran T=20°C; Grignard coupling reaction; 9 h;
参考文献
Inamoto, Kiyofumi; Kuroda, Jun-Ichi; Sakamoto, Takao; Hiroya, Kou
Synthesis, 2007 , # 18 p. 2853 - 2861
100-59-4
苯基氯化镁
+
530-93-8
β-四氢萘酮
→
反应条件
20669-52-7
反应条件
1: 1,2,3,4-tetrahydro-naphthalen-2-one With phosphorochloridic acid diphenyl ester; 2,4,6-trimethylphenylmagnesium bromide in tetrahydrofuran T=0 - 20°C; 1 h; 2: phenyl-magnesium chloride With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=65°C; 0.5 h;
参考文献
Miller, Joseph A.
Tetrahedron Letters, 2002 , vol. 43, # 39 p. 7111 - 7114
100-59-4
苯基氯化镁
+
93-55-0
苯丙酮
→
反应条件
2042-85-5
1,2-二(苯基)丙-1-酮
反应条件
1: phenyl-magnesium chloride With AlCl3, aluminium chloride in tetrahydrofuran 2: 1-phenyl-propan-1-one With dihydro-isoxazole in tetrahydrofuran; dichloromethane T=0 - 20°C;
参考文献
Miyoshi, Tetsuya; Sato, Shohei; Tanaka, Hiroya; Hasegawa, Chihiro; Ueda, Masafumi; Miyata, Okiko
Tetrahedron Letters, 2012 , vol. 53, # 32 p. 4188 - 4191
25187-00-2
+
100-59-4
苯基氯化镁
→
反应条件
1985-32-6
反应条件
1: phenyl-magnesium chloride in tetrahydrofuran; ethylene glycol dimethyl ether T=-20°C; 0.166667 h; 2: 2-iodobenzophenone With iron (III) acetylacetonate in tetrahydrofuran; ethylene glycol dimethyl ether T=-20 - 25°C; 0.5 h;
参考文献
Sapountzis, Ioannis; Lin, Wenwei; Kofink, Christiane C.; Despotopoulou, Christina; Knochel, Paul
Angewandte Chemie - International Edition, 2005 , vol. 44, # 11 p. 1654 - 1657
5162-03-8
+
100-59-4
苯基氯化镁
→
反应条件
1985-32-6
反应条件
manganese (II) chloride in tetrahydrofuran T=-5°C; 3 h;
参考文献
Cahiez, Gerard; Luart, Denis; Lecomte, Fabien
Organic Letters, 2004 , vol. 6, # 24 p. 4395 - 4398
100-59-4
苯基氯化镁
+
609-65-4
→
反应条件
1985-32-6
反应条件
1: phenyl-magnesium chloride With lithium chloride; manganese (II) chloride in tetrahydrofuran T=-30°C; 2: o-chloro benzoic acid chloride in tetrahydrofuran T=-30 - 0°C;
参考文献
Cahiez, Gerard; Luart, Denis; Lecomte, Fabien
Organic Letters, 2004 , vol. 6, # 24 p. 4395 - 4398
13047-06-8
+
100-59-4
苯基氯化镁
→
反应条件
1985-32-6
反应条件
1: phenyl-magnesium chloride in tetrahydrofuran; ethylene glycol dimethyl ether T=-20°C; 0.166667 h; 2: 2-bromobenzophenone With iron (III) acetylacetonate in tetrahydrofuran; ethylene glycol dimethyl ether
参考文献
Sapountzis, Ioannis; Lin, Wenwei; Kofink, Christiane C.; Despotopoulou, Christina; Knochel, Paul
Angewandte Chemie - International Edition, 2005 , vol. 44, # 11 p. 1654 - 1657
512787-24-5
+
100-59-4
苯基氯化镁
→
反应条件
1985-32-6
反应条件
1: phenyl-magnesium chloride in tetrahydrofuran; ethylene glycol dimethyl ether T=-20°C; 0.166667 h; 2: 2-benzoylphenyl trifluoromethanesulfonate With iron (III) acetylacetonate in tetrahydrofuran; ethylene glycol dimethyl ether
参考文献
Sapountzis, Ioannis; Lin, Wenwei; Kofink, Christiane C.; Despotopoulou, Christina; Knochel, Paul
Angewandte Chemie - International Edition, 2005 , vol. 44, # 11 p. 1654 - 1657
401-78-5
+
100-59-4
苯基氯化镁
→
反应条件
366-04-1
反应条件
[polymer-incarcerated nickel nanocatalyst] PICB–NHC–Ni (0.25 mol percent as Ni) in tetrahydrofuran T=20°C; 12 h;
参考文献
Soule, Jean-Francois; Miyamura, Hiroyuki; Kobayashi, Shu
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10602 - 10605
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