1: phenyl-magnesium chloride With titanium tetraethoxide in tetrahydrofuran
T=0°C;
2: 4-bromo-N,N-dimethyl-aniline With P[2,4,6-(OMe)3C6H2]3 in tetrahydrofuran
T=25°C; 16 h; Further stages.;
参考文献
Manolikakes, Georg; Dastbaravardeh, Navid; Knochel, Paul
Synlett, 2007 , # 13 p. 2077 - 2080
1: With iron (+/-)-(N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine)dichloride in tetrahydrofuran
T=-20°C; 0.25 h;
2: With LiH3BNMe2 in tetrahydrofuran
T=-20 - 20°C; 16 h;
参考文献
Le Bailly, Bryden A. F.; Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2012 , vol. 48, # 10 p. 1580 - 1582
