1: With acetic anhydride in acetonitrile T=0°C; 3 h; Molecular sieve; 2: With sodium tris(acetoxy)borohydride in acetonitrile T=0°C; 0.166667 h; Molecular sieve; Further stages;
1: N-methylaniline With n-butyllithium in tetrahydrofuran T=-40°C; 0.5 h; 2: With bis(cyclopentadienyl)zirconium monomethylmonochloride in tetrahydrofuran T=-50°C; 0.5 h; 3: vinyl 1-butyl ether in tetrahydrofuran T=80°C; 18 h; Further stages.;
参考文献
Barluenga, Jose; Rodriguez, Felix; Alvarez-Rodrigo, Lucia; Zapico, Jose M.; Fananas, Francisco J.
Chemistry - A European Journal, 2004 , vol. 10, # 1 p. 109 - 116
potassium carbonate in acetonitrile T=40°C; 20 h; Inert atmosphere;
参考文献
Orchard, Alexandra; Schamerhorn, Gregory A.; Calitree, Brandon D.; Sawada, Geri A.; Loo, Tip W.; Claire Bartlett; Clarke, David M.; Detty, Michael R.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 14 p. 4290 - 4302
