1: O-isopropyl N-methyl-N-phenylthiocarbamate With sulfuryl dichloride in chloroform-d1
T=25°C;
2: in chloroform-d1; methanol-d4
2 h;
3: N-methylaniline in chloroform-d1; methanol-d4
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
sulfuryl dichloride
1.) <2H>chloroform, 25 deg C, 10 min, 2.) chloroform, 25 deg C, 5 min; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Mott, Andrew W.; Barany, George
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2615 - 2621