1: 74 percent / t-butyllitium, TMEDA / pentane / -10 °C 2: n-butyllitium / tetrahydrofuran / 0.5 h / -50 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 25, # 5 p. 553 - 556
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反应条件
in acetonitrile Kinetics; byproducts: CH2O; stoicheiometric oxidation of N,N-dimethylaniline by the Ru complex in MeCN at 21°C; spectrophotometrical determination of the rate constant;
参考文献
Leising, Randolph A.; Ohman, Jeffrey S.; Acquaye, John H.; Takeuchi Kenneth J.
Journal of the Chemical Society, Chemical Communications, 1989 , # 14 p. 905 - 906