Banks, Ronald E.; Brown, Alan K.; Haszeldine, Robert N.; Jefferson, John
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1068 - 1070
Banks, Ronald E.; Brown, Alan K.; Haszeldine, Robert N.; Jefferson, John
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1068 - 1070
ClP(O)(OC2H5)2 in dimethyl sulfoxide
byproducts: C6H5OP(O)(OC2H5)2; anisol, Ph3SnNa and ClP(O)(OC2H5)2 in 1:2:2.4 ratio in DMSO; anisol, Ph3SnNa heated at 110°C for 12 h; ClP(O)(OC2H5)2 added; room temp., 24 h; sepd. by column chromy. on silica gel;
参考文献
Chopa, Alicia B.; Silbestri, Gustavo F.; Lockhart, Maria T.
Journal of Organometallic Chemistry, 2005 , vol. 690, # 17 p. 3865 - 3877