n-butyllithium in diethyl ether; hexane adding soln. of BuLi in hexane at 0°C to soln. of PhSMe in dry ether, refluxing soln. under stirring overnight, cooling to 0°C, adding Bu3SnCl in one portion, refluxing mixt. for 4 h, cooling to room temp.; partitioning react. mixt. between satd. brine and ether, sepn. of org. phase, drying over anhyd. MgSO4, evapn., flash chromy. (silica gel/hexane); elem. anal.;
参考文献
Li; Nishiwaki; Itami; Yoshida
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 9 p. 1717 - 1725
