2-甲酰基-3,4-二氢吡喃合成路线 (共 35 条)
反应条件
Na5P3O10; acetaldehyde; hydroquinone 0.0833333 h; Irradiation;
参考文献
Hsieh, Hsing-Pang; Chen, Shui-Tein; Wang, Kung-Tsung
Journal of the Chinese Chemical Society, 1997 , vol. 44, # 6 p. 597 - 600
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine -70 deg C; Multistep reaction;
参考文献
Chemische Berichte, , vol. 123, # 1 p. 153 - 168
反应条件
hydroquinone in benzene T=170°C; Diels-Alder reaction; 3 h; Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 30, # 7 p. 1159 - 1165
反应条件
1: 55 percent / DIBAL / tetrahydrofuran / 1 h / 0 °C 2: 1.) oxalyl chloride, DMSO, 2.) triethylamine / -70 deg C View Scheme
参考文献
Chemische Berichte, , vol. 123, # 1 p. 153 - 168
反应条件
in ethylene glycol dimethyl ether; benzene Diels-Alder reaction; KineticsMechanism; Temperature;
参考文献
Angewandte Chemie - International Edition, , vol. 48, # 48 p. 9156 - 9159
反应条件
E(activation); KineticsProduct distributionThermodynamic data;
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 60, # 3 p. 588 - 592,552 - 555
反应条件
1: Raney nickel / Hydrogenation 2: benzene; pyridine; phosphorus (III)-bromide View Scheme
参考文献
Servigne; Szarvasi
Bulletin de la Societe Chimique de France, 1956 , p. 1254,1256
反应条件
lithium aluminium tetrahydride in diethyl ether T=15°C; 1 h;
参考文献
Fehr, Charles; Galindo, Jose; Ohloff, Guenther
Helvetica Chimica Acta, 1981 , vol. 64, # 5 p. 1247 - 1256
反应条件
ethyltitanium triisopropoxide in diethyl ether -50 deg C to room temp. over 12 h; Yields of byproduct given;
参考文献
Singh, Shankar M.; Oehlschlager, Allan C.
Canadian Journal of Chemistry, 1988 , vol. 66, p. 209 - 213
反应条件
methanol; platinum Hydrogenation;
参考文献
Alder; Offermanns; Rueden
Chemische Berichte, 1941 , vol. 74, p. 927