1: With potassium hydroxide in benzene Etherification; 23 h; Heating; 2: With toluene-4-sulfonic acid in methanol; dichloromethane T=20°C; Ring cleavage; 5 h;
1: 2,2-dimethyl-1,3-dioxolane-4-methanol With sodium hydride in N,N-dimethyl-formamide; mineral oil 0.666667 h; Cooling with ice; 2: benzyl bromide in N,N-dimethyl-formamide; mineral oil T=20°C; 2 h;
参考文献
Chen, Chao-Yuan; Han, Wei-Bo; Chen, Hui-Jun; Wu, Yikang; Gao, Po
European Journal of Organic Chemistry, 2013 , # 20 p. 4311 - 4318
Doren, Henk A. van; Geest, Ralph van der; Kellogg, Richard M.; Wynberg, Hans
Recueil des Travaux Chimiques des Pays-Bas, 1990 , vol. 109, # 3 p. 197 - 203
