5-乙基-3(2H)-异噁唑酮合成路线 （共 4 条）
反应条件
hydrogenchloride in acetic acid Ambient temperature;
参考文献
Sato, Masayuki; Ogasawara, Hiromichi; Komatsu, Sachiko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3848 - 3856
反应条件
1: 61 percent / xylene / 0.75 h / Heating 2: 72 percent / H2 / 20percent Pd-C / ethanol / 3.5 h / 760 Torr / Ambient temperature 3: 54 percent / hydrogen chloride / acetic acid / Ambient temperature View Scheme
参考文献
Sato, Masayuki; Ogasawara, Hiromichi; Komatsu, Sachiko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3848 - 3856
反应条件
1: 72 percent / H2 / 20percent Pd-C / ethanol / 3.5 h / 760 Torr / Ambient temperature 2: 54 percent / hydrogen chloride / acetic acid / Ambient temperature View Scheme
参考文献
Sato, Masayuki; Ogasawara, Hiromichi; Komatsu, Sachiko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3848 - 3856
反应条件
1: 71 percent / toluene / 4 h / 65 °C 2: 88 percent / aq. HCl / methanol / 20 °C View Scheme
参考文献
Sorensen, Ulrik S.; Falch, Erik; Krogsgaard-Larsen, Povl
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1003 - 1007
