反应条件
Multi-step reaction with 3 steps 1: 68 percent / TiCl4, N-methylmorpholine / tetrahydrofuran; CCl4 / 22 h / 0 °C2: 73 percent / H2 / PtO2 / ethanol / 7 h / 100 °C / 76000 Torr3: 57 percent / NaH / dioxane / 1.) r.t., 4 h, 2.) reflux, 2 h
参考文献
Cook, Barry; Dingwall, John G. Phosphorus and Sulfur and the Related Elements, 1985 , vol. 22, p. 211 - 216
