Nε-三氟乙酰基-L-赖氨酸合成路线 （共 12 条）
反应条件
sodium in ethanol T=5 - 20°C;
参考文献
RETROTOPE, INC.
Patent: WO2009/114809 A1, 2009 ;
Location in patent: Page/Page column 7 ;
反应条件
in ethanol T=5 - 20°C;
参考文献
Russian Journal of Organic Chemistry, , vol. 43, # 10 p. 1427 - 1431
参考文献
Journal of the Chemical Society. Perkin transactions 1, , vol. 24, p. 2349 - 2359
反应条件
in 1,4-dioxane T=45°C; 2 h;
参考文献
Cherevin; Gulevich; Popova; Zubreichuk; Knizhnikov
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 10 p. 1427 - 1431
反应条件
in ethyl acetate T=70°C; 4 h;
参考文献
Huesmann, David; Birke, Alexander; Klinker, Kristina; Tuerk, Stephan; Raeder, Hans Joachim; Barz, Matthias
Macromolecules, 2014 , vol. 47, # 3 p. 928 - 936
反应条件
2,6,6-trimethylbicyclo[3.1.1]hept-2-ene in ethyl acetate T=105 - 110°C;
参考文献
Obeid, Rodolphe; Armstrong, Tracy; Peng, Xiaoju; Busse, Karsten; Kressler, Joerg; Scholz, Carmen
Journal of Polymer Science, Part A: Polymer Chemistry, 2014 , vol. 52, # 2 p. 248 - 257
反应条件
in tetrahydrofuran; N,N-dimethyl-formamide T=30°C; 2.5 h; Title compound not separated from byproducts;
参考文献
Blacklock; Shuman; Butcher; Shearin Jr.; Budavari; Grenda
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 836 - 844
反应条件
1: tetrahydrofuran / 2.5 h / 30 °C 2: 88 percent / tetrahydrofuran / 4 h / 25 °C View Scheme
参考文献
Blacklock; Shuman; Butcher; Shearin Jr.; Budavari; Grenda
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 836 - 844
反应条件
sodium hydrogencarbonate
参考文献
Moore; Rydon; Smithers
Journal of the Chemical Society. Perkin transactions 1, 1966 , vol. 24, p. 2349 - 2359
反应条件
1: tetrahydrofuran; dimethylformamide / 2.5 h / 30 °C 2: 94 percent Chromat. / tetrahydrofuran; H2O / 0.03 h / 0 - 12 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 53, # 4 p. 836 - 844
