3-氨基-2-羟基-N,N-二甲基苯甲酰胺盐酸盐合成路线 (共 2 条)
反应条件
1: With potassium ethanolate; hydrogen; palladium on activated carbon in ethanol P=6205.94 - 7757.43 Torr; 6 h; 2: With hydrogenchloride in water
参考文献
SCHERING CORPORATION
Patent: WO2009/5802 A1, 2009 ;
Location in patent: Page/Page column 25 ;
反应条件
1: With triethylamine in ethanol
T=0 - 10°C; 10 h;
2: With acetic acid in ethanol
T=0°C; 0.25 h; Heating / reflux; Product distribution / selectivity;
参考文献
SCHERING CORPORATION
Patent: WO2009/5801 A1, 2009 ;
Location in patent: Page/Page column 32 ;