反应条件
1-bromo-butane; water in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
soln. of Ph2GeK2 in HMPA/THF added to n-BuBr, stirred at room temp. for30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
参考文献
Mochida, Kunio; Matsushige, Naoki; Hamashima, Mari
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 5 p. 1443 - 1447
