1-氯-2-(2-氯乙基二硫基)乙烷合成路线 （共 30 条）
反应条件
pyridine; thionyl chloride in tetrahydrofuran 18 h; Ambient temperature;
参考文献
Allgeier, Alan M.; Slone, Caroline S.; Mirkin, Chad A.; Liable-Sands, Louise M.; Yap, Glenn P.A.; Rheingold, Arnold L.
Journal of the American Chemical Society, 1997 , vol. 119, # 3 p. 550 - 559
反应条件
(i) aq. H2O2, (ii) aq. HCl; Multistep reaction;
参考文献
Boehringer Ingelheim Pharmaceuticals, Inc.
Patent: US4692448 A1, 1987 ;
反应条件
hydrogenchloride in diethyl ether
参考文献
Kondo,K. et al.
Journal of the American Chemical Society, 1972 , vol. 94, # 16 p. 5786 - 5793
参考文献
Etlis,V.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1965 , vol. 35, # 3 p. 475 - 479,472 - 475
参考文献
Fuson et al.
Journal of Organic Chemistry, 1946 , vol. 11, p. 487,497
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Kinnear; Harley-Mason
Journal of the Society of Chemical Industry, London, 1948 , vol. 67, p. 108
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Pernot
Annales de Chimie (Cachan, France), 1946 , vol. <12>1, p. 635,638
反应条件
disulfur dichloride T=100°C;
参考文献
Guthrie
Justus Liebigs Annalen der Chemie, 1861 , vol. 119, p. 91
Justus Liebigs Annalen der Chemie, 1862 , vol. 121, p. 108
参考文献
Fuson et al.
Journal of Organic Chemistry, 1946 , vol. 11, p. 472
反应条件
chlorine; dibenzoyl peroxide
参考文献
Su,H.C.F. et al.
Journal of Organic Chemistry, 1961 , vol. 26, p. 4993 - 4995
反应条件
anhydrous methyl chloride; chlorine
参考文献
Wilson,G.E.; Huang,M.-G.
Journal of Organic Chemistry, 1976 , vol. 41, # 6 p. 966 - 968
反应条件
T=145 - 150°C; P=0.5 Torr;
参考文献
Pernot
Annales de Chimie (Cachan, France), 1946 , vol. <12>1, p. 635,638
